COURSE UNIT TITLE

: SAMPLING AND INSTRUMENTAL ANALYSIS IN CHEMICAL OCEANOGRAPHY - II

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
MCP 5010 SAMPLING AND INSTRUMENTAL ANALYSIS IN CHEMICAL OCEANOGRAPHY - II ELECTIVE 3 0 0 8

Offered By

Graduate School of Natural and Applied Sciences

Level of Course Unit

Second Cycle Programmes (Master's Degree)

Course Coordinator

Offered to

MARINE CHEMISTRY
MARINE CHEMISTRY

Course Objective

The aim of course is designed specifically for the instruction and use of analysts undertaking established or new chemical oceanographic analyses under operational conditions. Basic workings instructions are given in the fullest detail brief notes on the chemistry involved are included but only where this knowledge can contribute materially to the efficiency of the operator. All methods have had although trial under land or ship board laboratory conditions and a number of these methods constitutes a completely new application of analytical techniques to marine chemistry.

Learning Outcomes of the Course Unit

1   will be able to identify and describe the analytical principles and procedures of metals and organic compounds in marine environment of natural and anthropogenic activities which are responsible for marine pollution
2   will be able to describe the sampling design and sampling preparation techniques for particulate and soluble fractions
3   will be able to review the theory and application of instrumental methods of chemical analysis.
4   will be able to give the students further explanations on radioactive compounds

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Metals; Materials and cleaning procedures, sample handling, sample preservation and storage, metal pre-concentration methods
2 Analytical Methods; digestion methods, graphite furnace atomic absorption spectrometry (AAS)
3 Analytical Methods; Cold vapour AAS, Flame AAS
4 Analytical Methods; Inductively coupled plasma atomic emission spectrometry (ICP), voltametric methods, neutron activation analysis, X-ray fluorescence spectrometry
5 Organometallic compounds; Analysis of organometallic compounds, chemical speciation of organometallic compounds
6 Determination of major constituents; Analytical methods of Ca, Sr, Mg, Na, K.
7 Mid-term examination
8 Sample preparation prior to analysis for organics, the particulate fractions, the soluble fractions, volatile compounds
9 Organic compounds; Hydrocarbons, Organochlorine compounds
10 Polychlorinated biphenyls, lipids, sterols
11 Amino acids, carbohydrates, humic substances
12 Elemental analysis; Carbon, nitrogen, phosphorus
13 Application of mass spectrometric techniques to detection of natural and anthropogenic substances in the sea
14 Certified reference materials for chemical analysis in marine ecosystems

Recomended or Required Reading

-Course notes will be circulated during the class

-K. Grasshof, M. Ehrhardt, K. Kremling, Methods of Seawater Analysis, Second, Revised and Extended Edition, 1983, 418p.

-J.D.H. Stricland and T.R. Parsons, A Practical Handbook of Seawater Analysis, Bulletin 167 (Second edition), 1972, 310p.

-Analysis of Seawater, T.R. Compton,Butterworths&Co(Publishers)Ltd., 1989, 423p.

-Standard Methods for the Examination of Water and Wastewater, 15th Edition APHA-AWWA-WPCF, 1980, 1134p.

-TÜBITAK, 1989, Denizlerde Ölçüm ve Izleme Standart Yöntemler El Kitabı, Kalibrasyon I, Eds: A. Yılmaz, I. Salihoğlu, A. Acara ve T. Konuk.

Planned Learning Activities and Teaching Methods

The course is taught in a lecture and laboratory applications format. All class members are expected to attend both the lecture and take part in the laboratory and cruises
sessions.

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 FIN FINAL EXAM
3 FCG FINAL COURSE GRADE MTE * 0.50 + FIN * 0.50
4 RST RESIT
5 FCGR FINAL COURSE GRADE MTE * 0.50 + RST * 0.50


*** Resit Exam is Not Administered in Institutions Where Resit is not Applicable.

Further Notes About Assessment Methods

None

Assessment Criteria

To be announced.

Language of Instruction

Turkish

Course Policies and Rules

Reading the related parts of the course material each week, attending the course, laboratory applications and participating in class discussions are the requirements of
the course. Any unethical behavior that occurs either in presentations or in exams will be dealt with as outlined in school policy. Participation is obligatory 75% of lectures.

Contact Details for the Lecturer(s)

Prof. Dr. Filiz Küçüksezgin
Deniz Bilimleri ve Teknolojisi Enstitüsü
Inciraltı 35340, Izmir
Tel: 232-278 55 65/120
E mail: filiz.ksezgin@deu.edu.tr

Office Hours

Tuesday-Wednesday
10:00-12:00

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Lectures 13 2 26
Case study 13 1 13
Preparations before/after weekly lectures 13 2 26
Preparation for midterm exam 1 20 20
Preparation for final exam 1 20 20
Field study 2 45 90
Final 1 3 3
Midterm 1 3 3
TOTAL WORKLOAD (hours) 201

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11
LO.144343344434
LO.244343344433
LO.334343344433
LO.445343234443

CONTACT INFORMATION
Dokuz Eylül Üniversitesi Cumhuriyet Bulvarı No: 144 35210 Alsancak / İZMİR
Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

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