COURSE UNIT TITLE

: INSTRUMENTAL ANALYSIS LABORATORY

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 3020 INSTRUMENTAL ANALYSIS LABORATORY COMPULSORY 0 3 0 3

Offered By

Chemistry

Level of Course Unit

First Cycle Programmes (Bachelor's Degree)

Course Coordinator

PROFESSOR DOCTOR SERAP SEYHAN BOZKURT

Offered to

Chemistry
Chemistry (Evening)

Course Objective

The objective of this course is to perform applications of commonly used instrumental techniques of chemical analysis, to interpret the experimental results and to learn to submit the acquired data as a report

Learning Outcomes of the Course Unit

1   Students are expected to develop a full understanding of applications of instrumental techniques related to the lectures
2   Students are expected to choose the proper method considering the qualitative and quantitative expects of the analyte, are expected to plan the experimental procedure and can perform real applications
3   Students are expected to match their theoretical understanding with the experimental set up and the instruments
4   Students are expected to solve the problems regarding the analysis
5   Students can perform the necessary preparative applications and modifications on the sample

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Calibration line types
2 Performances characteristics of a spectrophotometer
3 Determination of molar absorption coefficient
4 Spectrophotometric determination of iron
5 Spectrophotometric determinaiton of mixture
6 Determination of fluorescein in antifreeze by fluorescence spectroscopy
7 Metal determinaiton by atomic absorption spectrometry
8 Midterm
9 Evaluation of midterm questions
10 Atomic emission spectroscopy: Ca and Mg analysis
11 FTIR: Comparison of sample preparation techniques and interpretation of the spectrum of the unknown
12 Determination of benzoic acid and salicyclic acid with FTIR
13 Thermogravimetric analysis of a metal oxalate hydrate
14 Compensation

Recomended or Required Reading

Lab experiment sheet

Planned Learning Activities and Teaching Methods

Interactive lecture, experimental application, report preparation

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 ASG ASSIGNMENT
3 FIN FINAL EXAM
4 FCGR FINAL COURSE GRADE (RESIT) MTE * 0.40 + ASG * 0.20 + FIN * 0.40
5 RST RESIT
6 FCGR FINAL COURSE GRADE (RESIT) MTE * 0.40 + ASG * 0.20 + RST * 0.40


*** Resit Exam is Not Administered in Institutions Where Resit is not Applicable.

Further Notes About Assessment Methods

None

Assessment Criteria

The student will be evaluated with a midterm exam, homework grade and final exam. The average of the grades obtained from the reports given after each experiment will be taken as the homework grade.

Language of Instruction

Turkish

Course Policies and Rules

It is the student's responsibility to attend 80% of the labs during the semester. Regarding unethical behaviors that may occur in labs, action will be taken within the framework of the relevant regulation. You can obtain the regulation on the teaching and examination application principles of the Faculty of Science at http://web.deu.edu.tr/fen.

Contact Details for the Lecturer(s)

melek.merdivan@deu.edu.tr
kadriye.ertekin@deu.edu.tr
ozlem.oter@deu.edu.tr
serap.seyhan@deu.edu.tr
mine.kurtbay@deu.edu.tr

Office Hours

To be announced.

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Tutorials 13 3 39
Preparations before/after weekly lectures 13 1 13
Preparation for midterm exam 1 3 3
Preparation for final exam 1 4 4
Preparing assignments 11 1 11
Midterm 1 2 2
Final 1 2 2
Quiz etc. 1 1 1
TOTAL WORKLOAD (hours) 75

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11PO.12PO.13PO.14PO.15PO.16PO.17
LO.14554
LO.255
LO.3555
LO.454
LO.53