COURSE UNIT TITLE

: INSTRUMENTAL ANALYSIS LABORATORY

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KMT 4204 INSTRUMENTAL ANALYSIS LABORATORY COMPULSORY 1 3 0 4

Offered By

Chemistry Technology

Level of Course Unit

Short Cycle Programmes (Associate's Degree)

Course Coordinator

PROFESSOR DOCTOR SUAT UÇAR

Offered to

Chemistry Technology
Chemistry Technology (Evening)

Course Objective

The aim of this course to describe the working principles of instrumental analysis equipments, to introduce parts of the device and to teach applications of the device to the students.

Learning Outcomes of the Course Unit

1   To be able to define potentiometric titration method and its applications.
2   To be able to perform qualitative and quantitative analysis of a mixture using gas chromatography device.
3   To be able to do analysis of heavy metals using atomic absorption spectroscopy device.
4   To be able to perform quantitative and qualitative analysis using ultraviolet and visible absorption spectroscopy device.
5   To be able to explain the importance of instrument device calibration while working with analysis instruments.

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Introduction to instrumental analysis laboratory, introduction of laboratory work rules and the device to be worked and the methods.
2 Introduction to electroanalytical chemistry, determination of acid by potentiometric titration.
3 Determination of pKa value of a weak acid by potentiometric titration.
4 Determination of an acid mixture by conductometric titration
5 Application of quanitative analysis by gas chromatography.
6 Application of quanitative analysis by gas chromatography.
7 Determination of copper in various drinks using atomic absorption spectrometry.
8 Mid-Term Exam
9 Determination of iron in drinking water samples using atomic absorption spectrometry.
10 Determination of manganese in drinking water using Ultraviolet-Visible spectrophotometry.
11 Determination of iron in drinking water by the spectrophotometric method.
12 Determination of the sugar percentage in aqueous sugar solution by measurement of the refractive index.
13 Determination of turbidity and sulphate ions in drinking water by turbidimetry.
14 Petroleum Products and Analysis Applications, ASTM distillation and flash point determination of diesel fuel
15 General repetition and compensation experiment.

Recomended or Required Reading

Textbook(s): Enstrümantal Analiz Ilkeleri Douglas A. Skoog, F. James Holler, Timothy A. Nieman, Translated by: Esma Kılıç, Bilim Yayıncılık, 2007.
Supplementary Book(s):
1. Enstrümantel Analiz, Turgut Gündüz, Gazi Kitabevi, 2005.
2. Enstrümantel Analiz, Emin Dikman, Çağlayan Kitabevi, 1985
Materials: Calculator, lab coat

Planned Learning Activities and Teaching Methods

1.Lecture
2.Laboratory Applications
3.Question-Answer

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 FN Final
3 FCG FINAL COURSE GRADE VZ*0.40 + FN* 0.60
4 RST RESIT
5 FCGR FINAL COURSE GRADE (RESIT) VZ*0.40 + BUT* 0.60


*** Resit Exam is Not Administered in Institutions Where Resit is not Applicable.

Further Notes About Assessment Methods

None

Assessment Criteria

The five learning outcomes will be assessed by mid-term and final exams.

Language of Instruction

Turkish

Course Policies and Rules

The students have to attend 70% of the courses and 80% of the application courses.
Any act of cheating will be resulted in disiplinary investigation.

Contact Details for the Lecturer(s)

Phone: 0232 - 3012613
E-mail: suat.ucar@deu.edu.tr; merve.zeyrek@deu.edu.tr;muge.hatip@deu.edu.tr

Office Hours

The appropriate office hours will be announced to the students at the beginning of the term.

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Lectures 14 1 14
Applications 14 3 42
Preparations before/after weekly lectures 14 2 28
Preparation for midterm exam 1 5 5
Preparation for final exam 1 10 10
Midterm 1 1 1
Final 1 1 1
TOTAL WORKLOAD (hours) 101

Contribution of Learning Outcomes to Programme Outcomes

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CONTACT INFORMATION
Dokuz Eylül Üniversitesi Cumhuriyet Bulvarı No: 144 35210 Alsancak / İZMİR
Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

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