COURSE UNIT TITLE

: MACROCYCLIC COMPOUNDS IN ANALYTICAL CHEMISTRY

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 6118 MACROCYCLIC COMPOUNDS IN ANALYTICAL CHEMISTRY ELECTIVE 3 0 0 8

Offered By

Graduate School of Natural and Applied Sciences

Level of Course Unit

Second Cycle Programmes (Master's Degree)

Course Coordinator

PROFESSOR DOCTOR SERAP SEYHAN BOZKURT

Offered to

Chemistry
Chemistry
Chemistry

Course Objective

The macrocyclic ligands play a very important role in analytical chemistry applications. These compounds such as porphyrin, crown ether, azacrown ether, thiacrown ether, calixarene complex with metal ions and interact with organic compounds and use in their separation and determination. The objective of this course is to introduce the application of each macrocyclic compound in analytical chemistry. Thus, in this course the importance and applications in the areas such as extraction and chromatography in analytical chemistry of each macrocylic compound will be discussed and explained in details.

Learning Outcomes of the Course Unit

1   Explain the each macrocyclic compounds and discuss the differences between chemical structures of these compounds
2   Examine the importance of macrocyclic compounds in analytical chemistry
3   Examine the usuability of macrocyclic compounds in the metal determination
4   Discuss the applications of macrocyclic compounds in the areas such as extraction and chromatography
5   Explain the sensitivity of macrocyclic compounds to metal ions

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Introduction to macrocyclic compounds: The classification of macrocyclic compounds, The properties of macrocyclic compounds
2 Macrocyclic coordination chemistry: Macrocyclic effect, Selectivity and efficiency of complexation
3 The metal extraction from the aqueous solution with macrocyclic compounds: Type of macrocyclic extractant, Efficiency of extraction with macrocyclic compounds
4 Porphyrins and applications of porphyrins in analytical chemistry: Importance of porphyrins and metal-porphyrin compounds, Spectroscopic properties of porphyrins and porphyrin-metal complexes, The use of porphyrins in the separation and determination of metal ions and organic molecules
5 Phthalocyanines and applications of phthalocyanines in analytical chemistry: Metal-phthalocyanine compounds, Spectroscopic properties of phthalocyanines and phthalocyanine-metal complexes, The use of phthalocyanines in the separation and determination of metal ions and organic molecules
6 Crown ethers and applications of crown ethers in analytical chemistry: Properties of crown ethers and metal-crown ether compounds, The use of crown ethers in the separation and determination of metal ions and organic molecules
7 Azacrown ethers, thiacrown ethers and applications of these compounds in analytical chemistry
8 Mid-term examination
9 Calixarenes and applications of calixarenes in analytical chemistry: Calixarene-metal compounds, The use of calixarenes in the separation and determination of metal ions and organic molecules
10 Other macrocyclic compounds containing heteroatom such as nitrogen, sulphur and their applications in analytical chemistry
11 Use of macrocyclic compounds impregnated or chemical bonded to support material in analytical chemistry
12 Applications of macrocyclic sorbents in chromatography, Metal determination in chromatography
13 Applications of macrocyclic sorbents in chromatography, Organic molecule determination in chromatography
14 Presentation of homework

Recomended or Required Reading

TEXTBOOK : Yury A. Zolotov, Macrocyclic Compounds in Analytical Chemistry, 1997.

REFERENCE BOOKS : T.W.Clarkson, Metals and their compounds in environment: occurance, analysis and biological relevance , Weinheim, N.Y. 1991.

Planned Learning Activities and Teaching Methods

1. Presentation
2. Question-answer technique
3. Homework

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 ASG ASSIGNMENT
3 FIN FINAL EXAM
4 FCG FINAL COURSE GRADE MTE *0.45 +ASG *0.10 +FIN *0.45
5 RST RESIT
6 FCGR FINAL COURSE GRADE (RESIT) MTE *0.45 +ASG *0.10 +BUT *0.45


*** Resit Exam is Not Administered in Institutions Where Resit is not Applicable.

Further Notes About Assessment Methods

None

Assessment Criteria

Student will be assessed with homework presentation and questions which will be asked in final exam.

Language of Instruction

Turkish

Course Policies and Rules

During the semester, the responsibility to continues 70% of the courses is student's self-owned. And must be observed the specified time about course times. Unethical behavior that may occur in class and on exams, will be acting within the framework of the relevant regulations. Teaching and examination implementation principles regulations of D.E.Ü Graduate School of Natural and Applied Sciences can be found at Graduate School of Natural and Applied Sciences web page.

Contact Details for the Lecturer(s)

DEU Science Faculty Chemistry Department
e-mail: serap.seyhan@deu.edu.tr

Office Hours

To be announced.

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Lectures 13 3 39
Preparations before/after weekly lectures 13 4 52
Preparation for midterm exam 1 30 30
Preparation for final exam 1 40 40
Preparing presentations 1 30 30
Midterm 1 2 2
Final 1 2 2
TOTAL WORKLOAD (hours) 195

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11
LO.134324355552
LO.233324343332
LO.33324343332
LO.423325355522
LO.52332433332

CONTACT INFORMATION
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Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

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