COURSE UNIT TITLE

: RECENT INNOVATIONS IN SOLID PHASE EXTRACTION

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 5129 RECENT INNOVATIONS IN SOLID PHASE EXTRACTION ELECTIVE 3 0 0 8

Offered By

Graduate School of Natural and Applied Sciences

Level of Course Unit

Second Cycle Programmes (Master's Degree)

Course Coordinator

PROFESSOR DOCTOR SERAP SEYHAN BOZKURT

Offered to

Chemistry
Chemistry
Chemistry

Course Objective

Solid phase extraction is analytical technique extensively used in separation and preconcentration of metal ions and organic molecules. The extraction efficiency of solid phase extraction depends on the type of sorbent used and interactions between the analyte and sorbent. The objective of this course is to present the recent innovations in the sorbents used as solid phase extractors for metal ions and organic molecules. The sorbents used in recent years in this purpose will be discussed in detail. The emphasis will be also given to application of several solid phase extraction systems for automated preparation of environmental, food and biological samples.

Learning Outcomes of the Course Unit

1   Examine the applications and principles of solid phase extraction method
2   Compare solid phase extraction method the other extraction methods
3   Explain the recent innovations in the sorbents used in solid phase extraction
4   Learn application of several solid phase extraction systems for automated preparation of environmental, food and biological samples
5   Explain the importance of solid phae extraction method in analytical chemistry

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Introduction to solid phase extraction: The solid phase extraction method, The steps solid phase extraction method, The columns used in the solid phase extraction method
2 The sorbents used in the solid phase extraction: Classic sorbents, Interactions between sorbent and analyte, Extraction efficiency with classic sorbents
3 Polymeric sorbents: Hydrophilic polymeric sorbents, Comparison of hydrophilic polymeric sorbents with classic sorbents
4 Polymeric sorbents: Polymeric sorbents, Interaction mechanism in the mixed-mode polymeric sorbents, Recovery with mixed-mode polymeric sorbents, Comparison of hydrophilic polymeric sorbents with classic sorbents
5 Molecularly imprinted polymers:Molecularly imprinted polymers
6 Molecularly imprinted polymers: Extraction efficiency with molecularly imprinted polymers, Comparison of molecularly imprinted polymeric sorbents with classic sorbents
7 Carbon nanotubes:Single-walled carbon nanotubes, Multi-walled carbon nanotubes, Sorption capacity of carbon nanotubes
8 Mid-term exam
9 Comparision of carbon nanotubes with activated carbon and C18 silica in terms of analytical performance
10 Admicelle and hemimicelle sorbents
11 Ionic liquids in solid phase extraction
12 Solid phase extraction systems for automated preparation of samples
13 On-line preconcentration
14 Presentation of homework

Recomended or Required Reading

TEXTBOOK : James Sherwood Fritz, Analytical solid phase extraction Wiley-VCH, 1999
Earl Michael Thurman, M. S. Mills, Solid phase extraction: principles and practice Wiley, 1998

REFERENCE BOOKS : Michael J. Telepchak, Thomas F. August, and Glynn Chaney, Forensic and clinical applications of solid phase extraction , 2004

Planned Learning Activities and Teaching Methods

1. presentation
2. question-answer technique
3. homework

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 ASG ASSIGNMENT
3 FIN FINAL EXAM
4 FCG FINAL COURSE GRADE MTE *0.45 +ASG *0.10 +FIN *0.45
5 RST RESIT
6 FCGR FINAL COURSE GRADE (RESIT) MTE *0.45 +ASG *0.10 +BUT *0.45


*** Resit Exam is Not Administered in Institutions Where Resit is not Applicable.

Further Notes About Assessment Methods

None

Assessment Criteria

Student will be assessed with homework presentation and questions which will be asked in mid-term exam and final exam.

Language of Instruction

Turkish

Course Policies and Rules

During the semester, the responsibility to continues 70% of the courses is student's self-owned. And must be observed the specified time about course times. Unethical behavior that may occur in class and on exams, will be acting within the framework of the relevant regulations. Teaching and examination implementation principles regulations of D.E.Ü Graduate School of Natural and Applied Sciences can be found at Graduate School of Natural and Applied Sciences web page.

Contact Details for the Lecturer(s)

DEÜ Science Faculty Chemistry Department
e-mail: serap.seyhan@deu.edu.tr

Office Hours

To be announced.

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Lectures 13 3 39
Preparations before/after weekly lectures 13 4 52
Preparation for midterm exam 1 30 30
Preparation for final exam 1 40 40
Preparing presentations 1 30 30
Midterm 1 2 2
Final 1 2 2
TOTAL WORKLOAD (hours) 195

Contribution of Learning Outcomes to Programme Outcomes

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LO.24435
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LO.443355533333
LO.55555555555

CONTACT INFORMATION
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Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

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