COURSE UNIT TITLE

: STRUCTURAL ANALYSIS TECHNIQUES OF NATURAL COMPOUNDS

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 6018 STRUCTURAL ANALYSIS TECHNIQUES OF NATURAL COMPOUNDS ELECTIVE 3 0 0 8

Offered By

Graduate School of Natural and Applied Sciences

Level of Course Unit

Second Cycle Programmes (Master's Degree)

Course Coordinator

Offered to

Chemistry
Chemistry
Chemistry

Course Objective

The aim of this course is to give isolation and purification techniques of classes of natural compounds from plants, chromatographic and spectroscopic methods used in their structural identification and innovations in these techniques.

Learning Outcomes of the Course Unit

1   Classify the natural Compounds
2   Have knowledge of the Isolation techniques for classes of natural compounds from plants
3   Have knowledge of the Purification techniques of classes of natural compounds
4   Have knowledge of chromatographic and spectroscopic methods used in structural identification of natural compounds
5   Follow the new developments and techniques in this field

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Classification of natural compounds, way of structural indentification
2 Flavonoids and chromatographic analysis; gas chromatography applications, UV and NMR spectral analyzes
3 Lipids, steroids, and chromatographic analysis
4 Alkaloids and their chromatographic and spectroscopic analyzes
5 Terpenoids and their chromatographic and spectroscopic analyzes
6 Carbohydrates and their chromatographic and spectroscopic analyzes
7 NMR technique in structural identification of complex compounds
8 Structural identification of natural compounds by using ` Chiroptical" features
9 NOE applications for determining distances between nuclei of natural compounds
10 Proton and C-13 determinations of biologically active natural compounds and modern 2D NMR techniques
11 Homework
12 Homework
13 Homework
14 Homework

Recomended or Required Reading

R. Ikan, Natural Products, Academic Press Inc. (London) , 1969.
Sanders J. K. M., Constable E. C. , Hunter B. K., Modern NMR Spectroscopy, Oxford University Press., London, 1989.
Supplementary Book(s): H. Duddeck, W. Dietrich, Structure Elucidation by Modern NMR, Steinkopff, Darmsdatt, NewYork, 1989
References:
Materials: Other natural compounds books, Ppt presentations which published on the internet

Planned Learning Activities and Teaching Methods

Presentation, describing the subject, question-answer, sampling, homework

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 ASG ASSIGNMENT
2 FIN FINAL EXAM
3 FCG FINAL COURSE GRADE ASG * 0.50 + FIN * 0.50
4 RST RESIT
5 FCGR FINAL COURSE GRADE (RESIT) ASG * 0.50 + RST * 0.50


*** Resit Exam is Not Administered in Institutions Where Resit is not Applicable.

Further Notes About Assessment Methods

None

Assessment Criteria

Student will be assessed with homework presentation and questions which will be asked in final exam.

Language of Instruction

Turkish

Course Policies and Rules

During the semester, the responsibility to continues 70% of the courses is student s self-owned. And must be observed the specified time about course times. Unethical behavior that may occur in class and on exams, will be acting within the framework of the relevant regulations. Teaching and examination implementation principles regulations of D.E.Ü Graduate School of Natural and Applied Sciences can be found at Graduate School of Natural and Applied Sciences web page.

Contact Details for the Lecturer(s)

yasar.yildiz@deu.edu.tr

Office Hours

Wednesday between 11-12 hours

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Lectures 10 3 30
Preparations before/after weekly lectures 10 3 30
Preparation for final exam 1 75 75
Preparing assignments 4 15 60
Final 1 4 4
TOTAL WORKLOAD (hours) 199

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11
LO.1543343
LO.2554535333
LO.3554535333
LO.455453533333
LO.555453533355

CONTACT INFORMATION
Dokuz Eylül Üniversitesi Cumhuriyet Bulvarı No: 144 35210 Alsancak / İZMİR
Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

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