COURSE UNIT TITLE

: INSTRUMENTAL ANALYSIS LABORATORY

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 3020 INSTRUMENTAL ANALYSIS LABORATORY COMPULSORY 0 3 0 3

Offered By

Chemistry

Level of Course Unit

First Cycle Programmes (Bachelor's Degree)

Course Coordinator

ASSOCIATE PROFESSOR HAYRIYE MINE ANTEP

Offered to

Chemistry
Chemistry (Evening)

Course Objective

The objective of this course is To gain skills in making, reporting and interpreting the results of experimental applications related to the approaches used in instrumental analysis.

Learning Outcomes of the Course Unit

1   Students are expected to develop a full understanding of applications of instrumental techniques related to the lectures
2   Students are expected to choose the proper method considering the qualitative and quantitative expects of the analyte, are expected to plan the experimental procedure and can perform real applications
3   Students are expected to match their theoretical understanding with the experimental set up and the instruments
4   Students are expected to solve the problems regarding the analysis
5   Students can perform the necessary preparative applications and modifications on the sample

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Determination of fluorescein in antifreeze by fluorescence spectroscopy
2 Determination of chlorophyll in olive oil by fluorescence spectroscopy
3 FTIR: Comparison of sample preparation techniques and interpretation of the spectrum of the unknown
4 Calibration line generation with direct and standard addition methods in atomic absorption spectroscopy
5 Metal determination by atomic absorption spectrometry
6 Atomic emission spectroscopy: Ca and Mg analysis
7 Thermogravimetric analysis of a metal oxalate hydrate
8 General evoluation of spectroscopy
9 Qualitative analysis of clove components by GC-MS
10 Quantitiative analysis with GC
11 Antibiotics analysis in HPLC
12 Polyfenolic compounds analysis in HPLC
13 Pigment analysis in TLC
14 General evoluation of chromatography

Recomended or Required Reading

Lab experiment sheet

Planned Learning Activities and Teaching Methods

Interactive lecture, experimental application, report preparation

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 ASG ASSIGNMENT
3 FIN FINAL EXAM
4 FCGR FINAL COURSE GRADE (RESIT) MTE * 0.40 + ASG * 0.20 + FIN * 0.40
5 RST RESIT
6 FCGR FINAL COURSE GRADE (RESIT) MTE * 0.40 + ASG * 0.20 + RST * 0.40


*** Resit Exam is Not Administered in Institutions Where Resit is not Applicable.

Further Notes About Assessment Methods

None

Assessment Criteria

Interactive lecture, experimental application, report preparation

Language of Instruction

Turkish

Course Policies and Rules

The student is obliged to attend the classes at a rate of 80% during the semester. Unethical behaviors that may occur in lessons and exams will be followed within the framework of the relevant regulations. You can obtain the DEU Faculty of Science regulation on teaching and exam application principles at http://web.deu.edu.tr/fen

Contact Details for the Lecturer(s)

melek.merdivan@deu.edu.tr
kadriye.ertekin@deu.edu.tr
ozlem.oter@deu.edu.tr
serap.seyhan@deu.edu.tr
mine.kurtbay@deu.edu.tr

Office Hours

To be announced.

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Tutorials 14 3 42
Preparations before/after weekly lectures 14 1 14
Preparation for midterm exam 1 4 4
Preparation for final exam 1 5 5
Preparing assignments 12 1 12
Midterm 1 1 1
Final 2 1 2
TOTAL WORKLOAD (hours) 80

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11PO.12PO.13PO.14PO.15PO.16PO.17
LO.14554
LO.255
LO.3555
LO.454
LO.53