Dokuz Eylül University Information Package / Courses Catalog

Description of Individual Course Units

Course Unit Code	Course Unit Title	Type Of Course	D	U	L	ECTS
KIM 6042	MASS SPECTROSCOPY	ELECTIVE	3	0	0	8

Offered By

Graduate School of Natural and Applied Sciences

Level of Course Unit

Second Cycle Programmes (Master's Degree)

Course Coordinator

PROFESSOR DOCTOR KADRIYE ERTEKIN

Offered to

Chemistry
Chemistry
Chemistry

Course Objective

The course aims to provide an introduction to mass spectrometry techniques, to give a detailed presentation of mass spectrometry especially in terms of , theoritical bases, interpretetion of a wide variaty of mass spectral data and its applications in chemical analysis.

Learning Outcomes of the Course Unit

1	This course is expected to help the students to provide an introduction to mass spectrometry techniques into detail in terms of instrumentation and theory, to make an assessment on analysis with mass spectroscopy
2	To develop the students analytical thinking abilities and to give the ability to criticize and solve problems regarding instrumental analysis with MS, correct desicions regarding chooise of instrument.
3	To give the students further information on interpertation of mass spectarl fragmants for a wide wariaty of organic compounds
4	To give the students further information on skills, pretreatment, and interpertation of mass spectral fragmants of samples regarding environmental, criminal, medical, drug, polymer and, new materials.
5	To give the students thinking abilitiy on comparison of MS based approachs, their advantages and disadvantagaes over each other, and making interpretation considering concequenses of the analysis.

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week	Subject	Description
1	Introduction to mass spectroscopy (MS), history and development of MS.
2	Instrumentation for MS.
3	Classification of MS methods considering instrumentataion and ionization techniquies, chooise of approrprate method for sample.
4	Theoric bases of interpretataion of mass spectarl fragmans.
5	Spectra of Alkanes, Alkenes, isotop effects
6	Spectar of aldehaydes, ketones and carboxylic acids.
7	Mc Lafferty rearrengement reactions
8	Aromatic compounds
9	Analysis and interpretataion of complex organic compounds
10	MS analysis of high molecular weight species
11	Analysis of drug, pestiside, steriod etc.
12	Student presentataion
13	Student presentataion
14	Student presentataion

Recomended or Required Reading

The mass spectrometry, ... R. M. Silverstein, F. X. Webster,; John Wiley &
Sons, 6th Edition, 1997.
1.Sparkman, O. David (2000). Mass spectrometry desk reference. Pittsburgh: Global View
Pub. ISBN 0-9660813-2-3.
2. Principles of Instrumental Analysis Douglas A. Skoog, F. James Holler and Timothy A.
Nieman Harcourt Brace College Publishers
3. Mass Spectrometry: Principles and Applications (2nd ed.),
Edmond de Hoffman; Vincent Stroobant (2001). John Wiley and Sons. ISBN 0-471-48566-7.
4. Price, Phil (1991). "Standard definitions of terms relating to mass spectrometry. A
report from the Committee on Measurements and Standards of the American Society for
Mass Spectrometry". Journal of the American Society for Mass Spectrometry 2 (4):
336 348. doi:10.1016/1044-0305(91)80025-3

Planned Learning Activities and Teaching Methods

Lecture, presentation, project

Assessment Methods

SORTING NUMBER	SHORT CODE	LONG CODE	FORMULA
1	PRS 1	PRESENTATION 1
2	PRS 2	PRESENTATION 2
3	FIN	FINAL EXAM
4	FCG	FINAL COURSE GRADE	PRS 1 * 0.20 + PRS 2 * 0.20 + FIN * 0.60
5	RST	RESIT
6	FCGR	FINAL COURSE GRADE (RESIT)	PRS 1 * 0.20 + PRS 2 * 0.20 + RST * 0.60

Further Notes About Assessment Methods

None

Assessment Criteria

The student will be assessed by the questions, homework and project.

Language of Instruction

English

Course Policies and Rules

Parallel shown on the website of the institute.

Contact Details for the Lecturer(s)

DEU Faculty of Science Department of Chemistry
e-mail: kadriye.ertekin@deu.edu.tr
Tel: 0 232 3018691
Prof. Dr. Kadriye Ertekin
Prof. Dr. Serap Alp

Office Hours

To be announced.

Work Placement(s)

None

Workload Calculation

Activities	Number	Time (hours)	Total Work Load (hours)
Presentataion by lecturer	13	3	39
Presentataion by students	3	3	9
Preparation before/after weekly lectures	1	20	20
Individual Assignments	2	20	40
Preparing lecture materials	12	5	60
Preparing presentataions or projects	1	30	30
Final exam	1	3	3
TOTAL WORKLOAD (hours)			201

Contribution of Learning Outcomes to Programme Outcomes

PO/LO	PO.1	PO.2	PO.3	PO.4	PO.5	PO.6	PO.7	PO.8	PO.9	PO.10	PO.11
LO.1	4	5	5	4	2	5	4	4	4	5	5
LO.2	4	5	5		2	5	4	4	4	5	5
LO.3	4	4			5	5	4	4	4	5	5
LO.4	5	5	5		5	5	4	3	4	5	5
LO.5	5			5	5	5	4	4	4	5	5

COURSE UNIT TITLE

DEGREE PROGRAMMES

Description of Individual Course Units

Offered By

Level of Course Unit

Course Coordinator

Offered to

Course Objective

Learning Outcomes of the Course Unit

Mode of Delivery

Prerequisites and Co-requisites

Recomended Optional Programme Components

Course Contents

Recomended or Required Reading

Planned Learning Activities and Teaching Methods

Assessment Methods

Further Notes About Assessment Methods

Assessment Criteria

Language of Instruction

Course Policies and Rules

Contact Details for the Lecturer(s)

Office Hours

Work Placement(s)

Workload Calculation

Contribution of Learning Outcomes to Programme Outcomes

CONTACT INFORMATION