COURSE UNIT TITLE

: NMR SPECTROSCOPY

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 5020 NMR SPECTROSCOPY ELECTIVE 3 0 0 8

Offered By

Graduate School of Natural and Applied Sciences

Level of Course Unit

Second Cycle Programmes (Master's Degree)

Course Coordinator

PROFESSOR DOCTOR GÜLSIYE ÖZTÜRK

Offered to

Chemistry
Chemistry
Chemistry

Course Objective

The aim of this course is to give every aspect of NMR spectroscopy.

Learning Outcomes of the Course Unit

1   The Students are expected to be able to: Have knowledge about the basic principles of magnetic resonance spectroscopy;
2   Have knowledge about 1H NMR and interpret spectra ;
3   Have knowledge about 13C NMR and interpret spectra ;
4   Have knowledge about Two-dimensional NMR.
5   Interpret 1H NMR and 13C NMR spectra together and learn what kind of information could be obtained about the structure.

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Basic Principles of Nuclear Magnetic Resonance Spectroscopy
2 Factors Affecting Proton Shift
3 Factors Affecting Chemical Shifts of Nuclei Other Than Proton
4 Coupling constant
5 1 H NMR spectra analysis
6 13C NMR Spectroscopy
7 Dynamic Processes, Effects of Relaxation
8 Multiple Beams, Nuclear Overhauser Effect (NOE)
9 Two-dimensional J-Differential Spectroscopy
10 Evaluation of 1H NMR and 13C NMR spectra together
11 Homework
12 Homework
13 Homework
14 Spectra Analysis

Recomended or Required Reading

Textbook(s): Prof.Dr.Kemal Yelekçi, Modern Nükleer Manyetik Rezonans Spektroskopisi ve Uygulamaları Istanbul Marmara Üniv. Yayınları 516, 1991.
Prof..Dr.Metin Balcı, Nükleer Manyetik Rezonans , METU PRESS Yayınları Ocak 2000.
Edwin D.Becker, High Resdution NMR (Theory and Chemical Applications), (Second Addition) Academic Press, 1980.
Supplementary Book(s): Abraham, P. Loftus, Proton and Carbon-13 NMR Spectroscopy, (An integrated Approach), Heyden and Sons Ltd. 1980.
Derek Shaw, Fourier Transform NMR Spectroscopy (Second Ed.) Elsevier Science Publishers B.V. Printed in The Netherlands, 1984.
Philip L. Fuchs, Chaarles A. Bunnel, Carbon-13 NMR Based Organic Spectral Problems John Wiley and Sons, US, 197
References:
Materials: Other NMR books, Ppt presentations which published on the internet

Planned Learning Activities and Teaching Methods

Pressentation, describing the subject, question-answer, sampling, homework

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 ASG ASSIGNMENT
2 FIN FINAL EXAM
3 FCG FINAL COURSE GRADE ASG * 0.50 + FIN * 0.50
4 RST RESIT
5 FCGR FINAL COURSE GRADE (RESIT) ASG * 0.50 + RST * 0.50


Further Notes About Assessment Methods

None

Assessment Criteria

Student will be assessed with homework presentation and questions which will be asked in final exam.

Language of Instruction

Turkish

Course Policies and Rules

During the semester, the responsibility to continues 70% of the courses is student s self-owned. And must be observed the specified time about course times. Unethical behavior that may occur in class and on exams, will be acting within the framework of the relevant regulations. Teaching and examination implementation principles regulations of D.E.Ü Graduate School of Natural and Applied Sciences can be found at Graduate School of Natural and Applied Sciences web page.

Contact Details for the Lecturer(s)

serap.alp@deu.edu.tr, gulsiye.ozturk@deu.edu.tr

Office Hours

Wednesday, Thursday 15.00-17.00

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Lectures 10 3 30
Preparations before/after weekly lectures 10 3 30
Preparation for final exam 1 75 75
Preparing assignments 3 20 60
Final 1 4 4
TOTAL WORKLOAD (hours) 199

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11
LO.133222232
LO.233222232
LO.333222232
LO.433222232
LO.533222232