COURSE UNIT TITLE

: ANALITICAL CHEMISTRY LABORATORY II

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 2030 ANALITICAL CHEMISTRY LABORATORY II COMPULSORY 0 0 3 4

Offered By

Chemistry

Level of Course Unit

First Cycle Programmes (Bachelor's Degree)

Course Coordinator

PROFESSOR DOCTOR SERAP SEYHAN BOZKURT

Offered to

Chemistry

Course Objective

To apply the quantitative analysis in the some samples according to the principle information of volumetric (precipitation, complexation, redox) or spectroscopic methods.

Learning Outcomes of the Course Unit

1   The experimental ways for quantitative analysis should be planned, applied and interpreted
2   The quantitative analysis in the real or laboratory sample should be planned and applied as volumetric by using titrations of precipitation, complexation and redox and the results should be evaluated
3   Should be able to determine the equivalence point potentiometrically in a volumetric analysis and evaluate the results.
4   Can make experimental planning by choosing a method for analysis according to the sample type.
5   Can solve problems encountered during analysis.

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

KIM 2033 - Analytical Chemistry Laboratory I

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Preparation of EDTA solution, determination of magnesium by direct titration
2 Determination of water hardness with EDTA
3 Determination of calcium and magnesium in the egg crust
4 Preparation of fixed permanganate solution and the determination of iron amount
5 Analysis of oxalate and bioxalate mixtures by permanganometry
6 Preparation of fixed thiosulfate solution and determination of copper amount (iodine based titrations)
7 Potentiometric acid-base titrations
8 Conductometric acid-base titrations
9 Calibration variants
10 Performance characteristics of a spectrophotometer
11 Phenanthroline method-spectrophotometric iron determination
12 Simultaneous determination of chromium and cobalt by visible absorption spectrophotometer
13 Determination of chlorophyll in olive oil by UV-Visible spectroscopy
14 Compensation

Recomended or Required Reading

Lab experiment sheet
Stanley Crouch, Donald West, F Holler, Douglas A. Skoog, "Skoog West Fundamentals Of Analytical Chemistry 9th Ed C.li", ISBN13 : 9780495558286, 2013.
F. James Holler , Stanley R. Crouch, "Enstrümantal Analiz Ilkeleri", ISBN :9789755560731, 2013.

Planned Learning Activities and Teaching Methods

Interactive expression, question-answer technique, experimental application and report

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 ASG ASSIGNMENT
3 FIN FINAL EXAM
4 FCG FINAL COURSE GRADE MTE * 0.40 + ASG * 0.20 + FIN * 0.40
5 RST RESIT
6 FCGR FINAL COURSE GRADE (RESIT) MTE * 0.40 + ASG * 0.20 + RST * 0.40


Further Notes About Assessment Methods

None

Assessment Criteria

The student will be evaluated with a midterm exam, homework grade and final exam. The average of the grades obtained from the reports given after each experiment will be taken as the homework grade.

Language of Instruction

Turkish

Course Policies and Rules

The student is obliged to attend 80% of the labs during the term. Unethical behaviors that may occur in the laboratories will be followed within the framework of the relevant regulation. You can obtain the DEU Faculty of Science regulation on teaching and exam application principles at http:/web.deu.edu.tr./fen

Contact Details for the Lecturer(s)

melek.merdivan@deu.edu.tr
kadriye.ertekin@deu.edu.tr
ozlem.oter@deu.edu.tr
serap.seyhan@deu.edu.tr
mine.kurtbay@deu.edu.tr

Office Hours

To be announced.

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Tutorials 14 3 42
Preparations before/after weekly lectures 14 1 14
Preparation for midterm exam 1 7 7
Preparation for final exam 1 9 9
Preparing assignments 13 2 26
Final 1 1 1
Midterm 1 1 1
TOTAL WORKLOAD (hours) 100

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11PO.12PO.13PO.14PO.15PO.16PO.17
LO.145
LO.25
LO.35
LO.455
LO.555

CONTACT INFORMATION
Dokuz Eylül Üniversitesi Cumhuriyet Bulvarı No: 144 35210 Alsancak / İZMİR
Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

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